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SiliCycle™ SiliaBond™ Functionalized Silica Gels, Pyridinium Chlorochromate (PCC), 40 to 63 μm, 60 Å
Powerful oxidizing agent that minimizes side reactions, greatly facilitates removal of Cr byproducts and is compatible with acid-sensitive protecting groups.
$68.10 - $3260.00
Specifications
| For Use With (Application) | Removal of Polymeric Reduced Chromium By-products |
|---|---|
| Particle Size | 40 to 63 μm |
| Product Type | Bulk Functionalized Irregular Silica Gel |
| Particle Shape | Irregular |
| Pore Size | 60 Å |
| Catalog Number | Mfr. No. | Quantity | Price | Quantity & Availability | |||||
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| Catalog Number | Mfr. No. | Quantity | Price | Quantity & Availability | |||||
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01-184-423
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SiliCycle™
R24030B10G |
10 g |
Each for $68.10
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01-184-357
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SiliCycle™
R24030B25G |
25 g |
Each for $141.80
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01-184-358
|
SiliCycle™
R24030B50G |
50 g |
Each for $256.50
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01-184-359
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SiliCycle™
R24030B100G |
100 g |
Each for $408.00
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01-184-360
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SiliCycle™
R24030B250G |
250 g |
Each for $957.00
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01-184-424
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SiliCycle™
R24030B500G |
500 g |
Each for $1,805.00
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01-184-361
|
SiliCycle™
R24030B1KG |
1 kg |
Each for $3,260.00
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01-184-356
|
SiliCycle™
R24030B5G |
5 g | Item Discontinued This item has been discontinued by the supplier. Please Sign In to view product availability in your area. | N/A | |||||
Description
SiliaBond™ Pyridinium Chlorochromate (Si-PCC) is used for the general oxidation of alcohols to carbonyl compounds, selective oxidation of allylic and benzylic alcohols, organometallic oxidation, oxidative transpositions, oxidative cleavages, allylic and benzylic oxidation, and oxidative cyclizations.
Using PCC immobilized onto silica gel provides anhydrous conditions that may otherwise promote side reactions and reduce yields. It greatly facilitates the removal of polymeric-reduced chromium byproducts and is compatible with acid-sensitive protecting groups. When used in conjunction with ultrasounds, kinetics are increased and the amount of oxidant required to complete the reaction is decreased.
Oxidation of 4-tert-butylcyclohexanol to 4-tert-butylcyclohexanone with 2 eq. in anhydrous DCM at room temperature is complete after 6 hours.
Specifications
| Removal of Polymeric Reduced Chromium By-products | |
| Bulk Functionalized Irregular Silica Gel | |
| 60 Å | |
| Pyridinium Chlorochromate (PCC) |
| 40 to 63 μm | |
| Irregular | |
| SiliaBond™ |
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